ChemicalBook CAS DataBase List N-HEXADECANE-D34

N-HEXADECANE-D34 synthesis

15synthesis methods

Product Name:N-HEXADECANE-D34
CAS Number:544-76-3
Molecular formula:C16H34
Molecular Weight:226.44

57-10-3 Synthesis

57-10-3
569 suppliers
$5.00/250mg

629-62-9 Synthesis

629-62-9
208 suppliers
$6.00/25g

544-76-3
287 suppliers
$6.00/25g

Yield:629-62-9 69.3% ，544-76-3 13.8%

Reaction Conditions:

with hydrogen in decane at 260; under 7500.75 Torr; for 4 h;Autoclave;Reagent/catalyst;Time;Pressure;

Steps:

1 Example 1 (Catalytic Reaction)

51.2 mg of palmitic acid, 42.5 mg of the catalyst 1 and 2 mL of decane were weighed, placed in an autoclave (model TVS-N 2 manufactured by Taiatsu techno corp.), and it was heated with a metal bath (manufactured by Koike precision instruments) while stirring with a magnetic stirrer under a hydrogen atmosphere. The reaction was conducted for 4 hours at a temperature of 260 ° C and a pressure of 1 MPa. (Analysis of Product) After the reaction, an internal standard substance (dodecane) was added to the reaction solution and the conversion (yield) (%) with respect to the raw material was derived by gas chromatographic analysis. The yield with respect to the raw material pentadecane, which is a linear hydrocarbon (B), was 69.3%, and the yield with respect to the raw material hexadecane, which is a linear hydrocarbon (A), was 13.8%. The molar ratio (B / A) was 5.0

References:

JP2018/16545,2018,A Location in patent:Paragraph 0034-0037

629-27-6 Synthesis