ChemicalBook CAS DataBase List Methyltrichlorosilane

Methyltrichlorosilane synthesis

14synthesis methods

Product Name:Methyltrichlorosilane
CAS Number:75-79-6
Molecular formula:CH3Cl3Si
Molecular Weight:149.47

Produced by Grignard reaction of silicon tetrachloride and methylmagnesium chloride.

74-87-3
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$18.50/48622

75-79-6
278 suppliers
$15.00/5 g

Yield:75-79-6 82.8%

Reaction Conditions:

with palladium silicide at 400 - 500; for 7.5 h;Product distribution / selectivity;Inert atmosphere;

Steps:

1
COMPARATIVE EXAMPLE 1[0059] A sample of Pd2Si (200.0 mg) was loaded into a flow-through, metal reactor and pretreated with nitrogen flow at 150 °C overnight. Next, MeCl (30 mL/min) was flowed through the catalyst bed continuously at reaction temperature of 400 °C for 4 h, 450 °C for 1.5 h, and 500 °C for 2 h. The remaining solids left in the tube were analyzed by ICP-AES, and the Si conversion was determined to be 82.8% (w/w). MeSiCl3 was the only

References:

DOW CORNING CORPORATION;ANDERSON, Kurt, E.;DASH, Aswini, K.;HALL, Charles, Alan;KATSOULIS, Dimitris;WINELAND, Jonathan, David WO2012/102957, 2012, A1 Location in patent:Page/Page column 10

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1185-55-3 Synthesis