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ChemicalBook CAS DataBase List METHYL 2-FLUORO-5-NITROBENZOATE
2965-22-2

METHYL 2-FLUORO-5-NITROBENZOATE synthesis

10synthesis methods
-

Yield: 210 mg (99%)

Reaction Conditions:

in hydrogenchloride;methanol

Steps:

77.A A.
A. Methyl 2-Fluoro-5-nitrobenzoate A solution of 2-fluoro-5-nitrobenzoic acid (200 mg, 1.08 mmol) in 0.7 M HCl in methanol was stirred for 5 h. The mixture was concentrated yielding 210 mg (99%) of the title compound; which was used without further purification.

References:

Eli Lilly and Company US6635657, 2003, B1

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