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ChemicalBook CAS DataBase List FMOC-D-PHG-OH
111524-95-9

FMOC-D-PHG-OH synthesis

3synthesis methods
2835-06-5 Synthesis
2-Amino-2-phenylacetic acid

2835-06-5
286 suppliers
$6.00/25g

102410-65-1 Synthesis
Fmoc-L-phenylglycine

102410-65-1
216 suppliers
$5.00/1g

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: sodium carbonate / water; 1,4-dioxane / Cooling with ice
1.2: 5 h / 20 °C
2.1: trifluoroacetic acid / isopropyl alcohol; hexane / 25 °C / Resolution of racemate

References:

Islam, Md. Fokhrul;Adhikari, Suraj;Paik, Man-Jeong;Lee, Wonjae [Bulletin of the Korean Chemical Society,2019,vol. 40,# 4,p. 332 - 338]

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