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88949-37-5

DPP RED synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: potassium carbonate; sodium iodide / acetone; 1,2-dimethoxyethane / 24 h / Reflux
2: ammonium acetate; acetic acid / 3 h / Reflux
3: sodium tert-pentoxide / 2 h / Inert atmosphere; Reflux

References:

Calvo-Castro, Jesus;Warzecha, Monika;Oswald, Iain D. H.;Kennedy, Alan R.;Morris, Graeme;McLean, Andrew J.;McHugh, Callum J. [Crystal Growth and Design,2016,vol. 16,# 3,p. 1531 - 1542]