DL-4-Chlorophenylglycine synthesis
- Product Name:DL-4-Chlorophenylglycine
- CAS Number:6212-33-5
- Molecular formula:C8H8ClNO2
- Molecular Weight:185.61
1073-67-2
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$7.00/5g
6212-33-5
318 suppliers
$6.00/5g
Yield:-
Steps:
Multi-step reaction with 3 steps
1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / water; acetone / 18 h / 0 - 20 °C / Inert atmosphere
2: acetic acid; sodium nitrite / water; acetonitrile / 18 h / 20 °C
3: (S)-2-amino-(2-chlorophenyl)ethanoic acid / water; acetonitrile / 36 h / 50 °C / Reflux; Inert atmosphere
References:
Inada, Haruki;Shibuya, Masatoshi;Yamamoto, Yoshihiko [Journal of Organic Chemistry,2020,vol. 85,# 17,p. 11047 - 11059]
6212-32-4
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6212-33-5
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32549-33-0
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6212-33-5
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7099-88-9
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$45.00/50mg
6212-33-5
318 suppliers
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24091-92-7
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$50.00/500 mg
6212-33-5
318 suppliers
$6.00/5g