Dimethyl isopropylmalonate synthesis
- Product Name:Dimethyl isopropylmalonate
- CAS Number:2917-78-4
- Molecular formula:C8H14O4
- Molecular Weight:174.19
67-56-1
758 suppliers
$9.00/25ml
201230-82-2
1 suppliers
inquiry
1680-29-1
0 suppliers
inquiry
2917-78-4
95 suppliers
inquiry
Yield:2917-78-4 16998 g
Reaction Conditions:
at 20; for 2 h;Large scale;
Steps:
3
Into the reactor in the compound 15000gA, 160gNi (CO) 4 / PdC (90/10) 6400g of methanol and, with stirring, was blown from the bottom of the reaction vessel 12000g monoxide; at room temperature, the reaction 2 hours. (In the course of the reaction may be employed, sodium dihydrogen phosphate / sodium phosphate buffering system to control the PH of the reaction system is 8 or less, may also be added such as sodium methoxide or sodium hydroxide to control the PH of the reaction system is 8 or less.) after completion of the reaction, the product was filtered to remove insoluble solid material system, distillation under reduced pressure to obtain 16998g product.
References:
CN105712876,2016,A Location in patent:Paragraph 0058; 0059; 0060; 0061; 0062
![Bicyclo[1.1.0]butane-2,2-dicarboxylic acid, 2,2-dimethyl ester](/CAS/20240320/GIF/102127-54-8.gif)
102127-54-8
0 suppliers
inquiry
2917-78-4
95 suppliers
inquiry
14035-96-2
73 suppliers
$18.00/1g
7298-16-0
1 suppliers
inquiry
