DIMETHYL ETHYLIDENEMALONATE synthesis
- Product Name:DIMETHYL ETHYLIDENEMALONATE
- CAS Number:17041-60-0
- Molecular formula:C7H10O4
- Molecular Weight:158.15
75-07-0
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$14.00/5mL
108-59-8
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$5.00/25g
17041-60-0
51 suppliers
$104.00/5g
Yield: 97%
Reaction Conditions:
Stage #1:malonic acid dimethyl ester with acetic anhydride;lithium bromide at 80; for 4 h;
Stage #2:acetaldehyde at 80; for 1 h;Knoevenagel condensation;
References:
Sylla, Maite;Joseph, Delphine;Chevallier, Emilie;Camara, Cheikhou;Dumas, Francoise [Synthesis,2006,# 6,p. 1045 - 1049]
75-07-0
422 suppliers
$14.00/5mL
108-59-8
598 suppliers
$5.00/25g
17041-60-0
51 suppliers
$104.00/5g
1000210-73-0
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