Cyclopentane-1,1-diacetic acid synthesis
- Product Name:Cyclopentane-1,1-diacetic acid
- CAS Number:16713-66-9
- Molecular formula:C9H14O4
- Molecular Weight:186.21
4167-77-5
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16713-66-9
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C / Inert atmosphere
2.1: triethylamine / dichloromethane / 0.5 h / Inert atmosphere; Cooling
2.2: -3 - 20 °C / Inert atmosphere
3.1: N,N-dimethyl-formamide / 100 °C / Inert atmosphere
4.1: water; sodium hydroxide / ethanol / Inert atmosphere; Reflux
References:
BETA PHARMA CANADA INC;ASTAR BIOTECH LLC;WANG, Zhaoyin;LI, Lianhai WO2013/185202, 2013, A1
21079-25-4
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16713-66-9
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82683-51-0
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5763-53-1
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62161-65-3
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16713-66-9
147 suppliers
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