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ChemicalBook CAS DataBase List CMDA
122665-73-0

CMDA synthesis

5synthesis methods
32677-01-3 Synthesis
L-Glutamic acid di-tert-butyl ester hydrochloride

32677-01-3
228 suppliers
$6.00/1g

CMDA

122665-73-0
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: Et3N / CH2Cl2
2: H2 / 10percent Pd/C
3: 78 percent / acetic acid / 48 h / Ambient temperature
4: 0.3 percent / pyridine / 1.) 2 deg C, 20 min, 2.) 80 deg C, 80 min
5: 82 percent / trifluoroacetic acid / 0.5 h / Ambient temperature

References:

Springer, Caroline J.;Antoniw, Pari;Bagshawe, Kenneth D.;Searle, Frances;Bisset, Graham M. F.;Jarman, Michael [Journal of Medicinal Chemistry,1990,vol. 33,# 2,p. 677 - 681]

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