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ChemicalBook CAS DataBase List Cinnamyl chloride
2687-12-9

Cinnamyl chloride synthesis

11synthesis methods
Cinnamyl chloride is used in condiments, alcohol, candy, meat, and used as a raw material for preservatives and fungicides. It was prepared from styrene with formaldehyde by stirring in hydrochloric acid heated under reflux for 3h.
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: diisobutylaluminium hydride / tetrahydrofuran / -78 - 20 °C
2: thionyl chloride / dichloromethane / 0 - 20 °C

References:

Tian, Qinqin;Liu, Yulong;Wang, Xiaoyun;Wang, Xie;He, Wei [European Journal of Organic Chemistry,2019,vol. 2019,# 24,p. 3850 - 3855]

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