CINNAMALDEHYDE DIETHYL ACETAL synthesis
- Product Name:CINNAMALDEHYDE DIETHYL ACETAL
- CAS Number:7148-78-9
- Molecular formula:C13H18O2
- Molecular Weight:206.28
621-63-6
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 1.) oxalyl chloride, DMSO, 2.) triethylamine / tetrahydrofuran / 1.) -30 deg C, 15 min, 2.) - 60 deg C --> room temperature, room temperature, 1 h
2: 45 percent / nBuLi / tetrahydrofuran / 1.) -60 deg C to room temperature, 2.) room temperature, 3 h
References:
Bernard, Didier;Doutheau, Alain;Gore, Jacques [Synthetic Communications,1987,vol. 17,# 15,p. 1807 - 1814]
