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ChemicalBook CAS DataBase List Atractylodin
55290-63-6

Atractylodin synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: n-BuLi / tetrahydrofuran; hexane / 2 h / -78 - 20 °C
1.2: 54 percent / tetrahydrofuran; hexane / -78 - 20 °C
2.1: 59 percent / manganese dioxide / CH2Cl2 / 20 °C
3.1: 58 percent / PPh3 / CH2Cl2 / 20 °C
4.1: 72 percent / n-BuLi / hexane / 0.5 h / -78 - -40 °C

References:

Shi Shun, Annabelle L. K.;Tykwinski, Rik R. [Journal of Organic Chemistry,2003,vol. 68,# 17,p. 6810 - 6813]

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