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ChemicalBook CAS DataBase List ALPHA-NAPHTHYL ACRYLATE
20069-66-3

ALPHA-NAPHTHYL ACRYLATE synthesis

3synthesis methods
-

Yield:20069-66-3 95%

Reaction Conditions:

with magnesium hydroxide;di-tert-butyl dicarbonate;lithium carbonate at 50; for 6 h;Temperature;Reagent/catalyst;

Steps:

49-51 Example 36

General procedure: In a 1 L capacity eggplant-shaped flask, 153.370 grams (1629.69 mmol) of 6 phenol, 140.300 grams (1629.69 mmol) of 7 methacrylic acid, 362.938 grams (1629.69 mmol) of 8 di-t-butyl dicarbonate, 0.027 grams (0.65 mmol, 0.04 mol %) of 9 lithium hydroxide monohydrate, and 0.010 grams (0.16 mmol, 0.01 mol %) of 30 magnesium hydroxide were added successively. Then reaction was carried out at 25° C. while the mixture was stirred. Accordingly, 11 phenyl methacrylate was produced. The reaction result obtained 48 hours after the start of reaction is shown in Table 5.

References:

US2018/354885,2018,A1 Location in patent:Paragraph 0075; 0076

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