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ChemicalBook CAS DataBase List ALPHA-METHYL-L-TRYPTOPHAN
16709-25-4

ALPHA-METHYL-L-TRYPTOPHAN synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 5 steps
1: CF3COOH / 96 h / Ambient temperature
2: Na2CO3 / dioxane; H2O / 0 °C
3: 1.) lithium bis(trimethylsilyl)amide / 1.) THF, -78 deg C, 1 h, 2.) THF, a) -78 deg C, 1 h, b) from -78 deg C to RT, 2 h
4: trifluoroacetic acid / 1.5 h / Ambient temperature
5: H2 / 10percent Pd/C / ethanol / 3 h / Ambient temperature

References:

Ekhato, I. Victor;Huang, Yun [Journal of labelled compounds and radiopharmaceuticals,1997,vol. 39,# 12,p. 1019 - 1038]

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