ALPHA,ALPHA-DIMETHYLBENZYL CHLORIDE synthesis
- Product Name:ALPHA,ALPHA-DIMETHYLBENZYL CHLORIDE
- CAS Number:934-53-2
- Molecular formula:C9H11Cl
- Molecular Weight:154.64
Yield:-
Reaction Conditions:
in water;isopropenylbenzene
Steps:
10 EXAMPLE 10
The organic layer and aqueous layer were separated, and the aqueous layer was washed in water and dried over sodium sulfate, followed by filtering off the desiccant and distillation of the residue under reduced pressure to give 993 g of a mixture of α-methylstyrene and α,α-dimethylbenzyl alcohol. On analysis of the mixture by means of gas chromatography, the yields based on α,α-dimethylbenzyl chloride were 34.4% (441 g) in the case of α-methylstyrene and 37.4% (552 g) in the case of α,α-dimethylbenzyl alcohol. In the residue there was obtained 880 g of the intended N-(α,α-dimethylbenzylthio-carbonyl) hexamethyleneimine.
References:
Mitsubishi Petrochemical Co., Ltd. US4298740, 1981, A
617-94-7
196 suppliers
$6.00/1g
934-53-2
46 suppliers
$45.00/50mg
4148-93-0
2 suppliers
$57.00/1ea
934-53-2
46 suppliers
$45.00/50mg
13740-70-0
4 suppliers
inquiry
934-53-2
46 suppliers
$45.00/50mg
617-94-7
196 suppliers
$6.00/1g
65-85-0
1371 suppliers
$10.00/25 g
98-83-9
305 suppliers
$10.00/25mL
98-83-9
305 suppliers
$10.00/25mL
934-53-2
46 suppliers
$45.00/50mg