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99114-72-4

AKOS BC-1112 synthesis

2synthesis methods
-

Yield:-

Reaction Conditions:

in ethanol; for 1.16667 h;

Steps:

10

The N-(3-methylaminopropyl)morpholine, used as a starting material, was obtained by bubbling methylamine gas for 10 minutes through a solution of 3-morpholinopropyl chloride (3.27 g) in ethanol (30 ml). The resultant mixture was allowed to stand for 1 hour and then evaporated. The residual oil was triturated under diethyl ether and the resultant solid was dried under vacuum. There was thus obtained the required starting material (1.58 g).

References:

EP1226126,2005,B1 Location in patent:Page 36

AKOS BC-1112 Related Search: