Acethydrazide synthesis
- Product Name:Acethydrazide
- CAS Number:1068-57-1
- Molecular formula:C2H6N2O
- Molecular Weight:74.08
79-20-9
554 suppliers
$14.00/100g
1068-57-1
395 suppliers
$6.00/5g
Yield:1068-57-1 98%
Reaction Conditions:
with hydrazine hydrate at 40 - 75; for 4 h;Green chemistry;Large scale;Temperature;
Steps:
1.1 Example 1 Preparation of pymetrozine.
(1) Preparation of hydrazide:1000 g of methyl acetate (solvent) was put into a 3000 ml three-necked flask,Under stirring conditions,500 g of hydrazine hydrate was slowly added dropwise to the three-necked flask, and the dropping time was controlled to 2 hours. The temperature of the reaction solution was controlled to 40 to 45C.After the dropwise addition, the temperature was raised to 75 ° C for 4 h. Cooled to room temperature,After solidification and crystallization (cooling to below 0 ° C) to give solid acetylHydrazine 725 g, yield: 98%.
References:
Jiangsu Anbang Electrochemistry Co., Ltd.;Ji Yuxiang;Jiang Yutian;Yao Xiuyu;Wang Junsheng;Long Xiguo;Zheng Chen;Xie Jun CN103724327, 2017, B Location in patent:Paragraph 0006; 0030; 0031; 0036; 0037; 0038; 0039
141-78-6
634 suppliers
$20.50/250ml
1068-57-1
395 suppliers
$6.00/5g
64-19-7
1564 suppliers
$10.00/25ML
1068-57-1
395 suppliers
$6.00/5g
2208-07-3
155 suppliers
$6.00/5g
1068-57-1
395 suppliers
$6.00/5g
