(3S)-3-[4-[(5-Bromo-2-chlorophenyl)methyl]phenoxy]tetrahydrofuran synthesis
- Product Name:(3S)-3-[4-[(5-Bromo-2-chlorophenyl)methyl]phenoxy]tetrahydrofuran
- CAS Number:915095-89-5
- Molecular formula:C17H16BrClO2
- Molecular Weight:367.66
21739-92-4
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915095-89-5
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / fluorobenzene / 2 h / 15 - 25 °C
2: aluminum (III) chloride / 1 h / 0 - 25 °C
3: potassium tert-butylate / tetrahydrofuran / 0.5 h / 7 - 10 °C
4: aluminum (III) chloride; 1,1,3,3-Tetramethyldisiloxane / toluene / 2.5 h / 0 - 23 °C
References:
Wang, Xiao-Jun;Zhang, Li;Byrne, Denis;Nummy, Larry;Weber, Dirk;Krishnamurthy, Dhileep;Yee, Nathan;Senanayake, Chris H. [Organic Letters,2014,vol. 16,# 16,p. 4090 - 4093]
915095-85-1
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915095-89-5
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13888-04-5
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915095-89-5
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21900-52-7
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915095-89-5
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462-06-6
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915095-89-5
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