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ChemicalBook CAS DataBase List (2-fluoro-6-iodophenyl)carbaMic acid tert-butyl ester
908600-92-0

(2-fluoro-6-iodophenyl)carbaMic acid tert-butyl ester synthesis

4synthesis methods
-

Yield:908600-92-0 79%

Reaction Conditions:

Stage #1: tert-butyl 2-fluorophenylcarbamatewith carbon dioxide;tert.-butyl lithium in tetrahydrofuran;pentane at -78 - -20; for 1.5 h;
Stage #2: with iodine in tetrahydrofuran;pentane at 20;Further stages.;

References:

Jensen, Thomas;Pedersen, Henrik;Bang-Andersen, Benny;Madsen, Robert;Jorgensen, Morten [Angewandte Chemie - International Edition,2008,vol. 47,# 5,p. 888 - 890]

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(2-fluoro-6-iodophenyl)carbaMic acid tert-butyl ester

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