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23418-91-9

9-Borabicyclo[3.3.1]nonane,9-phenyl- synthesis

8synthesis methods
-

Yield:23418-91-9 81%

Reaction Conditions:

in tetrahydrofuran;diethyl ether;byproducts: H2; Ar-atmosphere; dropwise addn. of PhLi in Et2O to 9-BBN in THF (0°C), dropwise addn. of CH3SO3H; distn.;

References:

Kalbarczyk, E.;Pasynkiewicz, S. [Journal of Organometallic Chemistry,1985,vol. 292,p. 119 - 132]