9,10-dihydro-9,10-diphenylanthracene-9,10-diol synthesis

9synthesis methods

Product Name:9,10-dihydro-9,10-diphenylanthracene-9,10-diol
CAS Number:6318-17-8
Molecular formula:C26H20O2
Molecular Weight:364.44

108-86-1 Synthesis

108-86-1
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$10.00/5g

84-11-7 Synthesis

84-11-7
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$5.00/1g

9,10-dihydro-9,10-diphenylanthracene-9,10-diol

6318-17-8
5 suppliers
$28.60/25mg

Yield:6318-17-8 45%

Reaction Conditions:

with magnesium in tetrahydrofuran;1,4-dioxane;Grignard Reaction;

Steps:

9,10-Diaryl-9,10-dihydroanthracene-9,10-diols 6a and 6c; GeneralProcedure

General procedure: Diols 6a and 6c were synthesized via reaction of the Grignard reagentprepared from the appropriate aryl bromide (8 mmol) andmagnesium turnings (192 mg, 8 mmol) in THF (30 mL) with 9,10-anthraquinone (416 mg, 2 mmol) in 1,4-dioxane (60 mL).

References:

Periasamy, Mariappan;Beesu, Mallesh;Shanmugaraja, Masilamani [Synthesis,2013,vol. 45,# 20,art. no. SS-2013-Z0331-OP,p. 2913 - 2918]

108-86-1 Synthesis

108-86-1
511 suppliers
$10.00/5g