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ChemicalBook CAS DataBase List 1,3-Dihydro-3,3-dimethyl-1-(trifluoromethyl)-1,2-benziodoxole, Tognis Reagent
887144-97-0

1,3-Dihydro-3,3-dimethyl-1-(trifluoromethyl)-1,2-benziodoxole, Tognis Reagent synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: diethyl ether / 3 h / 0 - 23 °C / Inert atmosphere
1.2: 1 h / 23 °C / Inert atmosphere
2.1: acetonitrile / 16 h / 23 °C / Inert atmosphere; Darkness
3.1: cesium fluoride / acetonitrile / 16 h / 23 °C / Inert atmosphere; Darkness

References:

Powers, David C.;Lee, Eunsung;Ariafard, Alireza;Sanford, Melanie S.;Yates, Brian F.;Canty, Allan J.;Ritter, Tobias [Journal of the American Chemical Society,2012,vol. 134,# 29,p. 12002 - 12009]

81290-20-2 Synthesis
(Trifluoromethyl)trimethylsilane

81290-20-2
408 suppliers
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175786-58-0 Synthesis
1,2-Benziodoxole, 1-(acetyloxy)-1,3-dihydro-3,3-dimethyl

175786-58-0
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