ChemicalBook CAS DataBase List 7-NITRO-QUINOLINE

7-NITRO-QUINOLINE synthesis

14synthesis methods

Product Name:7-NITRO-QUINOLINE
CAS Number:613-51-4
Molecular formula:C9H6N2O2
Molecular Weight:174.16

3054-95-3 Synthesis

3054-95-3
205 suppliers
$28.00/25g

99-09-2 Synthesis

99-09-2
9 suppliers
$14.00/1g

613-51-4
119 suppliers
$8.00/250mg

Yield: 25.8 %Chromat.

Reaction Conditions:

with Ni-modified Beta zeolite in neat (no solvent) for 0.0833333 h;Microwave irradiation;Reflux;Green chemistry;

Steps:

2.2. Catalytic performance evaluation
General procedure: General procedure for synthesis of quinolines from anilines and ADA was carried out in Panasonic NN-K5541JF microwave oven reactor equipping a magnetic stirring device. The typical procedures were as follows: ADA (1mmol), excessive anilines (4mmol) and solid catalyst were charged into a round-bottom ask; and then, the mixtures was placed into microwave reactor. The reaction was conducted by continuous microwave irradiation for 1-40 min under refluxing and stirring condition. Finally, the resulting products were determined by GC-MS of Varian Saturn 2200/ CP-3800 gas chromatography-mass spectrometry equipped with two CP8944 capillary columns (VF-5,30m×0.25mm×0.25 μm).

References:

Li, An;Yang, Zan;Yang, Tao;Luo, Cai-Wu;Chao, Zi-Sheng;Zhou, Cong-Shan [Catalysis Communications,2018,vol. 115,p. 21 - 25]

30450-62-5 Synthesis