(1R)-trans-4-[N-Boc-1-aminoethyl]cyclohexanecarboxylic Acid synthesis
- Product Name:(1R)-trans-4-[N-Boc-1-aminoethyl]cyclohexanecarboxylic Acid
- CAS Number:671815-99-9
- Molecular formula:C14H25NO4
- Molecular Weight:271.35
24424-99-5
863 suppliers
$13.50/25G
149004-75-1
2 suppliers
inquiry
671815-99-9
27 suppliers
$165.00/10mg
Yield:671815-99-9 89%
Reaction Conditions:
Stage #1: trans-(R)-4-(1-aminoethyl)cyclohexanecarboxylic acidwith sodium hydroxide in tetrahydrofuran;water at 0; for 0.5 h;
Stage #2: di-tert-butyl dicarbonate in tetrahydrofuran;water at 20; for 48 h;
Stage #3: with hydrogenchloride in water; for 3 - 4 h;
References:
Paleek, Jii;Zweigerdt, Robert;Olmer, Ruth;Martin, Ulrich;Kirschning, Andreas;Draeger, Gerald [Organic and Biomolecular Chemistry,2011,vol. 9,# 15,p. 5503 - 5510] Location in patent:experimental part
3886-69-9
580 suppliers
$14.00/25G
671815-99-9
27 suppliers
$165.00/10mg
36283-44-0
46 suppliers
$85.00/500mg
671815-99-9
27 suppliers
$165.00/10mg
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88146-37-6
17 suppliers
$112.50/250mg
671815-99-9
27 suppliers
$165.00/10mg
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859163-61-4
13 suppliers
$155.00/500mg
671815-99-9
27 suppliers
$165.00/10mg