6-Isopropylpyridin-3-ol synthesis
- Product Name:6-Isopropylpyridin-3-ol
- CAS Number:101870-78-4
- Molecular formula:C8H11NO
- Molecular Weight:137.18
55717-45-8
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / dichloromethane / 48 h / 20 °C / Inert atmosphere
2: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / 1,4-dioxane / 90 °C / Inert atmosphere
3: 10 wt% Pd(OH)2 on carbon; hydrogen / ethanol / 20 °C
References:
Westaway, Susan M.;Preston, Alex G. S.;Barker, Michael D.;Brown, Fiona;Brown, Jack A.;Campbell, Matthew;Chung, Chun-Wa;Drewes, Gerard;Eagle, Robert;Garton, Neil;Gordon, Laurie;Haslam, Carl;Hayhow, Thomas G.;Humphreys, Philip G.;Joberty, Gerard;Katso, Roy;Kruidenier, Laurens;Leveridge, Melanie;Pemberton, Michelle;Rioja, Inma;Seal, Gail A.;Shipley, Tracy;Singh, Onkar;Suckling, Colin J.;Taylor, Joanna;Thomas, Pamela;Wilson, David M.;Lee, Kevin;Prinjha, Rab K. [Journal of Medicinal Chemistry,2016,vol. 59,# 4,p. 1370 - 1387]
1196074-40-4
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101870-78-4
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630120-99-9
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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101870-78-4
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1000210-73-0
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101870-78-4
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