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ChemicalBook CAS DataBase List 6-CHLORO-3-METHOXY-2-METHYLPYRIDINE
129692-13-3

6-CHLORO-3-METHOXY-2-METHYLPYRIDINE synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 90 percent / POCl3, PCl5 / 1 h / 140 °C
2: 90 percent / Pd(PPh3)4 / dioxane; hexane / 5.5 h / Heating
3: 90 percent / NaBO3 / acetic acid / 5.5 h / 80 °C
4: 15 percent / POCl3 / 1 h / Heating

References:

Ohta, Akihiro;Takahashi, Nobuhiro;Shirokoma, Yasuko [Heterocycles,1990,vol. 30,# 2,p. 875 - 884]

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