6-BROMO-4-HYDROXY-2-(TRIFLUOROMETHYL)QUINOLINE synthesis
- Product Name:6-BROMO-4-HYDROXY-2-(TRIFLUOROMETHYL)QUINOLINE
- CAS Number:1701-22-0
- Molecular formula:C10H5BrF3NO
- Molecular Weight:292.05
372-31-6
478 suppliers
$5.00/10g
106-40-1
476 suppliers
$12.00/5g
1701-22-0
91 suppliers
$40.00/250mg
Yield:-
Reaction Conditions:
Stage #1:ethyl 4,4,4-trifluoroacetoacetate;4-bromo-aniline with magnesium sulfate;acetic acid in ethanol at 90; for 16 h;
Stage #2: with dowtherm A at 230 - 250; for 0.5 h;
References:
Yang, Guan-Zhou;Zhu, Jia-Kai;Yin, Xiao-Dan;Yan, Yin-Fang;Wang, Yu-Ling;Shang, Xiao-Fei;Liu, Ying-Qian;Zhao, Zhong-Min;Peng, Jing-Wen;Liu, Hua [Journal of Agricultural and Food Chemistry,2019,vol. 67,# 41,p. 11340 - 11353]