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ChemicalBook CAS DataBase List 2-(4-METHOXYPHENYL)-4,4-DIMETHYL-4,5-DIHYDRO-1,3-OXAZOLE
53416-46-9

2-(4-METHOXYPHENYL)-4,4-DIMETHYL-4,5-DIHYDRO-1,3-OXAZOLE synthesis

12synthesis methods
-

Yield:53416-46-9 95%

Reaction Conditions:

Stage #1: 2-Amino-2-methyl-1-propanol;1-(4-methoxybenzoyl)-1H-1,2,3-benzotriazole in chloroform at 80; under 206.859 - 517.148 Torr; for 0.166667 h;microwave irradiation;
Stage #2: with thionyl chloride in chloroform at 80; for 0.0333333 h;microwave irradiation;

References:

Katritzky, Alan R.;Cai, Chunming;Suzuki, Kazuyuki;Singh, Sandeep K. [Journal of Organic Chemistry,2004,vol. 69,# 3,p. 811 - 814]

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