4-CHLORO-2,6-DIPHENYLPYRIMIDINE synthesis

4synthesis methods

Product Name:4-CHLORO-2,6-DIPHENYLPYRIMIDINE
CAS Number:29509-91-9
Molecular formula:C16H11ClN2
Molecular Weight:266.72

3740-92-9 Synthesis

3740-92-9
231 suppliers
$8.00/10g

98-80-6 Synthesis

98-80-6
740 suppliers
$5.00/5g

29509-91-9
137 suppliers
$16.00/1g

Yield: 75%

Reaction Conditions:

with tetrakis(triphenylphosphine) palladium⁽⁰⁾;tetrabutylammomium bromide;sodium hydroxide in water;toluene at 80; for 12 h;Inert atmosphere;

Steps:

8.1 1) Synthesis of Intermediate 1-38-2:
According to the synthesis method of compound 1-3-3, (12.2g, 100mmol) of compound 1-23-3 and (22.5g, 100mmol) of compound 1-38-1 were substituted for compound 1-3-1 and compound 1- 3-2, the yield is 75%.

References:

Guangzhou Huarui Optoelectric Materials Co., Ltd.;He Ruifeng;Huang Hong;Wu Canjie;Song Jingyao CN111848590, 2020, A Location in patent:Paragraph 0251-0256

3764-01-0 Synthesis