4-azabicyclo[3.1.1]heptane-5-carboxylic acid synthesis
- Product Name:4-azabicyclo[3.1.1]heptane-5-carboxylic acid
- CAS Number:1169708-23-9
- Molecular formula:C7H11NO2
- Molecular Weight:141.17
1169708-25-1
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1169708-23-9
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: acetic acid; zinc / Reflux; Inert atmosphere
2: triethylamine / methanol / 110 °C / Inert atmosphere
3: hydrogenchloride; water / Reflux; Inert atmosphere
4: palladium 10% on activated carbon; hydrogen / methanol / 3750.38 Torr
References:
De Blieck, Ann;Stevens, Christian V. [Synlett,2011,# 12,p. 1748 - 1752]
![2-(Phenylmethyl)-2-azabicyclo-[3.1.1]heptane-1-carbonitrile](/CAS/GIF/1169708-27-3.gif)
1169708-27-3
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1169708-23-9
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![2-benzyl-2-aza-bicyclo[3.1.1]heptane-1-carboxylic acid hydrochloride](/CAS/20180703/GIF/1334330-32-3.gif)
1334330-32-3
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1169708-23-9
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$411.00/100mg
1169708-26-2
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1169708-23-9
10 suppliers
$411.00/100mg