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ChemicalBook CAS DataBase List 4,4,5,5,5-pentafluoropentane-1-thiol
148757-88-4

4,4,5,5,5-pentafluoropentane-1-thiol synthesis

5synthesis methods
-

Yield:-

Reaction Conditions:

in N,N-dimethyl acetamide at 80; for 16 h;

Steps:

13

Example 13; Preparation of Cp 9304 from Cp 9342 (Depicted in FIG. 10); 40 grams of Cp 9360 (prepared according to Example 11) were heated at 80° C. for 16 hours with 14.8 grams of thiourea and 345 grams of dimethylacetamide to give 400 grams of a 10% solution of Cp 9383.

References:

US2006/30552,2006,A1 Location in patent:Page/Page column 25

172032-07-4 Synthesis
2-Penten-1-ol, 4,4,5,5,5-pentafluoro-2-iodo-

172032-07-4
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4,4,5,5,5-pentafluoropentane-1-thiol

148757-88-4
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