4-(2-METHOXY-5-METHYLPHENYL)-3-THIOSEMICARBAZIDE synthesis
1synthesis methods
- Product Name:4-(2-METHOXY-5-METHYLPHENYL)-3-THIOSEMICARBAZIDE
- CAS Number:71058-34-9
- Molecular formula:C9H13N3OS
- Molecular Weight:211.28
Yield:71058-34-9 60%
Reaction Conditions:
Stage #1: carbon disulfide;Cresidinewith ammonia in ethanol;water; for 1 h;
Stage #2: with hydrazine hydrate in ethanol;Heating;
References:
Hirpara;Parikh;Merja;Parekh [Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry,2003,vol. 42,# 5,p. 1172 - 1175]