3-Methyl-6-hepten-1-ol synthesis
- Product Name:3-Methyl-6-hepten-1-ol
- CAS Number:4048-32-2
- Molecular formula:C8H16O
- Molecular Weight:128.21
109-49-9
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 78 percent / trimethylsilyl chloride / CHCl3 / 1 h / Ambient temperature
2: 1.) lithium 4,4'-di-tert-butylbiphenylide / 1.) THF, -78 deg C, 10 min, 2.) THF, -78 deg C to room temp.
3: 1.) n-BuLi, lithium 4,4'-di-tert-butylbiphenylide, 2.) MeOH / 1.) THF, hexane, -78 deg C, 10 min, 2.) THF, hexane, -78 deg C
References:
Chen, Fangping;Mudryk, Boguslaw;Cohen, Theodore [Tetrahedron,1994,vol. 50,# 45,p. 12793 - 12810]
![Benzene, 1,1'-[(1-methyl-4-pentenylidene)bis(thio)]bis-](/CAS/20210305/GIF/161145-63-7.gif)
161145-63-7
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