3-bromo-2,6-difluorobenzoic acid synthesis
- Product Name:3-bromo-2,6-difluorobenzoic acid
- CAS Number:28314-81-0
- Molecular formula:C7H3BrF2O2
- Molecular Weight:237
372-18-9
422 suppliers
$9.00/1g
28314-81-0
112 suppliers
$7.00/100mg
Yield:-
Steps:
Multi-step reaction with 3 steps
1: 94 percent / butyllithium; bromine / hexane; tetrahydrofuran / 0.75 h / -75 °C
2: diisopropylamine; butyllithium / hexane; tetrahydrofuran / 2 h / -75 °C
3: 96 percent / 2,2,6,6-tetramethylpiperidine; butyllithium / hexane; tetrahydrofuran / 2 h / -75 °C
References:
Schlosser, Manfred;Heiss, Christophe [European Journal of Organic Chemistry,2003,# 23,p. 4618 - 4624]
348-57-2
419 suppliers
$5.00/5g
124-38-9
129 suppliers
$175.00/23402
28314-81-0
112 suppliers
$7.00/100mg
64248-56-2
275 suppliers
$6.00/1g
124-38-9
129 suppliers
$175.00/23402
28314-81-0
112 suppliers
$7.00/100mg
64248-56-2
275 suppliers
$6.00/1g
28314-81-0
112 suppliers
$7.00/100mg
348-57-2
419 suppliers
$5.00/5g
124-38-9
129 suppliers
$175.00/23402
28314-81-0
112 suppliers
$7.00/100mg
1583-58-0
422 suppliers
$6.00/5g
385-00-2
422 suppliers
$5.00/5g