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6962-57-8

3,6-DIHYDROXY-2,4-DIMETHOXYACETOPHENONE synthesis

12synthesis methods
Preparation by Fries rearrangement of 1,4-diacetoxy- 2,6-di-methoxybenzene with aluminium chloride in nitrobenzene at r.t.
-

Yield:6962-57-8 92 %

Reaction Conditions:

with boron trifluoride diethyl etherate in chloroform at 0 - 70;

References:

Kwon, Sangil;Lee, Sanha;Hur, Joonseong;Ko, Keebeom;Fei, Xiang;Jeong, Kwang Won;Sishtla, Kamakshi;Muniyandi, Anbukkarasi;Bae, Munhyung;Corson, Timothy W.;Seo, Seung-Yong [Journal of Natural Products,2023,vol. 86,# 1,p. 149 - 156] Location in patent:supporting information

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