3,6-BIS(DECYL)PHTHALONITRILE synthesis
- Product Name:3,6-BIS(DECYL)PHTHALONITRILE
- CAS Number:119931-48-5
- Molecular formula:C28H44N2
- Molecular Weight:408.66
4733-50-0
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 2,6-dimethylpyridine / dichloromethane / 14 h / -20 - 20 °C / Inert atmosphere
2: lithium chloride; potassium phosphate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / tetrahydrofuran / 10 h / 20 °C / Inert atmosphere; Reflux
References:
Heeney, Martin J.;Al-Raqa, Shaya A.;Auger, Aurélien;Burnham, Paul M.;Cammidge, Andrew N.;Chambrier, Isabelle;Cook, Michael J. [Journal of Porphyrins and Phthalocyanines,2013,vol. 17,# 8-9,p. 649 - 664]
