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ChemicalBook CAS DataBase List 3,5-DIMETHOXYPHENYLGLYOXAL HYDRATE
188199-78-2

3,5-DIMETHOXYPHENYLGLYOXAL HYDRATE synthesis

3synthesis methods
-

Yield:188199-78-2 77%

Reaction Conditions:

with hydrogen bromide in dimethyl sulfoxide at 60 - 68; for 8 h;

References:

Song, Zhiguo;DeMarco, Anthony;Zhao, Mangzhu;Corley, Edward G.;Thompson, Andrew S.;McNamara, James;Li, Yulan;Rieger, Dale;Sohar, Paul;Mathre, David J.;Tschaen, David M.;Reamer, Robert A.;Huntington, Martha F.;Ho, Guo-Jie;Tsay, Fuh-Rong;Emerson, Khateeta;Shuman, Richard;Grabowski, Edward J. J.;Reider, Paul J. [Journal of Organic Chemistry,1999,vol. 64,# 6,p. 1859 - 1867]

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