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ChemicalBook CAS DataBase List 3,5-DIIODOTOLUENE
49617-79-0

3,5-DIIODOTOLUENE synthesis

3synthesis methods
-

Yield:49617-79-0 73%

Reaction Conditions:

Stage #1: 1,2,3-triiodo-5-methylbenzenewith tert.-butyl lithium in tetrahydrofuran at -78; for 1 h;
Stage #2: with ethanol in tetrahydrofuran; for 24 h;regioselective reaction;

References:

Al-Zoubi, Raed M.;Futouh, Hassan Abul;McDonald, Robert [Australian Journal of Chemistry,2013,vol. 66,# 12,p. 1570 - 1575]

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