3,5-DIIODOTOLUENE synthesis
- Product Name:3,5-DIIODOTOLUENE
- CAS Number:49617-79-0
- Molecular formula:C7H6I2
- Molecular Weight:343.93
89677-87-2
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49617-79-0
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Yield:49617-79-0 73%
Reaction Conditions:
Stage #1: 1,2,3-triiodo-5-methylbenzenewith tert.-butyl lithium in tetrahydrofuran at -78; for 1 h;
Stage #2: with ethanol in tetrahydrofuran; for 24 h;regioselective reaction;
References:
Al-Zoubi, Raed M.;Futouh, Hassan Abul;McDonald, Robert [Australian Journal of Chemistry,2013,vol. 66,# 12,p. 1570 - 1575]
64662-57-3
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49617-79-0
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106-49-0
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49617-79-0
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