3',5'-DI-O-BENZOYL-5-FLUORO-2'-O-METHYLURIDINE synthesis

1synthesis methods

Product Name:3',5'-DI-O-BENZOYL-5-FLUORO-2'-O-METHYLURIDINE
CAS Number:158966-44-0
Molecular formula:C24H21FN2O8
Molecular Weight:484.43

22224-41-5 Synthesis

22224-41-5
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3',5'-DI-O-BENZOYL-5-FLUORO-2'-O-METHYLURIDINE

158966-44-0
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 71 percent / CH₂N₂, BF₃*OEt₂ / CH₂Cl₂ / 0.5 h / 4 °C
2: 68 percent / trimethylsilyl trifluoromethanesulfonate / acetonitrile / 0.5 h / Ambient temperature

References:

Ross;Springer;Vasquez;Andrews;Cook;Acevedo [Journal of Heterocyclic Chemistry,1994,vol. 31,# 4,p. 765 - 769]

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