N(6)-(delta(2)-isopentenyl)adenosine 5'-monophosphate synthesis
- Product Name:N(6)-(delta(2)-isopentenyl)adenosine 5'-monophosphate
- CAS Number:20268-93-3
- Molecular formula:C15H22N5O7P
- Molecular Weight:415.34
2004-06-0
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 70 percent / toluene-p-sulphonic acid monohydrate / 16 h / 20 °C
2: 79 percent / triethylamine / butan-1-ol / 3 h / Heating
3: pyridine, N-methylimidazole / dioxane / 1 h
4: 1.) H2O, pyridine, 2.) aq. HCl / 2.) 20 deg C, 15h
References:
Shadid, Belal;Plas, Henk C. van der [Tetrahedron,1990,vol. 46,# 3,p. 901 - 912]
