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ChemicalBook CAS DataBase List 2-DICYCLOHEXYLPHOSPHINO-2',6'-DIISOPROPOXYBIPHENYL
787618-22-8

2-DICYCLOHEXYLPHOSPHINO-2',6'-DIISOPROPOXYBIPHENYL synthesis

2synthesis methods
79128-08-8 Synthesis
1,3-DIISOPROPOXYBENZENE, 97%

79128-08-8
91 suppliers
$6.00/1g

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-BuLi / hexane / 2.5 h / Heating
1.2: hexane / 1.83 h / Heating
2.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C
2.2: 2.24 percent / tetrahydrofuran; hexane / -78 - 20 °C

References:

Milne, Jacqueline E.;Buchwald, Stephen L. [Journal of the American Chemical Society,2004,vol. 126,# 40,p. 13028 - 13032]

16523-54-9 Synthesis
Dicyclohexylchlorophosphine

16523-54-9
264 suppliers
$8.00/1g

870703-70-1 Synthesis
2-BROMO-2',6'-DIISOPROPOXY-1,1'-BIPHENYL

870703-70-1
15 suppliers
$73.90/5g

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