2-Diphenylphosphino-2'-(N,N-dimethylamino)biphenyl synthesis
- Product Name:2-Diphenylphosphino-2'-(N,N-dimethylamino)biphenyl
- CAS Number:240417-00-9
- Molecular formula:C26H24NP
- Molecular Weight:381.45
583-55-1
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240417-00-9
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 92 percent / NaOAc / Pd(OAc)2 / N,N-dimethyl-acetamide / 72 h / 130 °C
2: 100 percent / H2O2 / methanol / 1 h / 20 °C
3: 66 percent / PPh3; K3PO4 / Pd(dba)2 / dioxane / 48 h / 105 °C
4: 72 percent / trichlorosilane; triethylamine / toluene / 120 °C
References:
Baillie, Colin;Xiao, Jianliang [Tetrahedron,2004,vol. 60,# 19,p. 4159 - 4168]
![[1,1'-Biphenyl]-2-amine, 2'-(diphenylphosphinyl)-N,N-dimethyl-](/CAS/20210305/GIF/712350-51-1.gif)
712350-51-1
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240417-00-9
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88652-74-8
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4559-70-0
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829-85-6
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240417-00-9
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