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ChemicalBook CAS DataBase List 2-Diphenylphosphino-2'-(N,N-dimethylamino)biphenyl
240417-00-9

2-Diphenylphosphino-2'-(N,N-dimethylamino)biphenyl synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: 92 percent / NaOAc / Pd(OAc)2 / N,N-dimethyl-acetamide / 72 h / 130 °C
2: 100 percent / H2O2 / methanol / 1 h / 20 °C
3: 66 percent / PPh3; K3PO4 / Pd(dba)2 / dioxane / 48 h / 105 °C
4: 72 percent / trichlorosilane; triethylamine / toluene / 120 °C

References:

Baillie, Colin;Xiao, Jianliang [Tetrahedron,2004,vol. 60,# 19,p. 4159 - 4168]

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