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ChemicalBook CAS DataBase List 2-BROMOBENZO[B]THIOPHENE
5394-13-8

2-BROMOBENZO[B]THIOPHENE synthesis

5synthesis methods
-

Yield:5394-13-8 81%

Reaction Conditions:

Stage #1:Benzo[b]thiophene with sodium 2,2,6,6-tetramethylpiperidide in hexane at 25; for 0.5 h;
Stage #2: with 1,1,2,2-tetrabromoethane in hexane at -78; for 1 h;

Steps:

8.7 Experiment Number 7
General procedure: Benzo[b]thiophene was used as an arene, and 1,1,2,2-tetrabromoethane (Br2HCCHBr2) was used as an electrophilic reagent. The arene was reacted with Na-TMP in the same manner as in Experiment Number 2, the electrophilic reagent was added thereto and reacted therewith at -78° C. for 1 hour, the product was then evaluated, and the yield of isolated 2-bromo-benzo[b]thiophene in which a bromo group (-Br) was added at 2-position of benzo[b]thiophene was calculated. The isolated yield was 81%.

References:

KOBELCO ECO-SOLUTIONS CO.,LTD.;MURAKAMI, Yoshiaki;FUKUSHIMA, Miyuki;TAKAI, Kazuhiko;ASAKO, Sobi US2019/359571, 2019, A1 Location in patent:Paragraph 0127; 0130; 0131; 0140; 0141

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