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41964-65-2

2-BROMO-N-(3-CHLORO-PHENYL)-ACETAMIDE synthesis

5synthesis methods
A clean iodine flask of 250 ml was taken. 10ml  solution of freshly prepared 10% solution of sodium  carbonate was added to the flask followed by the  addition of 0.1 ml of 3- chloro aniline. Shake the flask  to mix it properly. Then bromoacetyl bromide was  added gradually. Again shake it vigorously until ppts  appeared. Precipitates were filtered and proper washing was done. Dry the precipitates and product  purity was checked by TLC. Amount was calculated & packed.
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Yield:41964-65-2 100%

Reaction Conditions:

with triethylamine in dichloromethane at 0; for 1.25 h;Inert atmosphere;

References:

Leung, Euphemia;Hung, Joy M.;Barker, David;Reynisson, Johannes [MedChemComm,2014,vol. 5,# 1,p. 99 - 106]

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