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ChemicalBook CAS DataBase List 2-BROMO-4 6-DIMETHYLPHENYL ISOCYANATE
78831-81-9

2-BROMO-4 6-DIMETHYLPHENYL ISOCYANATE synthesis

1synthesis methods
201230-82-2 Synthesis
carbon monoxide

201230-82-2
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1-Bromo-3,5-dimethyl-2-nitrobenzene

78831-77-3
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Yield:78831-81-9 50%

Reaction Conditions:

bis(tetrahydrofurane)oxovanadium(IV) dichloride;(Bu4N) in 1,2-dichloro-benzene at 120; under 750.06 Torr;Rate constant;

References:

Tietz, Helmut;Schwetlick, Klaus [Zeitschrift fur Chemie,1985,vol. 25,# 4,p. 149 - 150]

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