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ChemicalBook CAS DataBase List 2-AMINOMETHYL-3-(4-FLUORO-PHENYL)-PROPIONIC ACID
910443-83-3

2-AMINOMETHYL-3-(4-FLUORO-PHENYL)-PROPIONIC ACID synthesis

3synthesis methods
72707-66-5 Synthesis
2-(BROMOMETHYL)ACRYLIC ACID

72707-66-5
99 suppliers
$72.00/250mg

459-45-0 Synthesis
4-FLUOROBENZENEDIAZONIUM TETRAFLUOROBORATE

459-45-0
27 suppliers
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2-AMINOMETHYL-3-(4-FLUORO-PHENYL)-PROPIONIC ACID

910443-83-3
15 suppliers
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Yield:-

Reaction Conditions:

Stage #1: 2-(bromomethyl)acrylic acidwith ammonia in water at 20; for 17 h;
Stage #2: 4-fluorobenzenediazonium tetrafluoroboratewith hydrogenchloride;titanium(III) chloride in water at 40; for 0.583333 h;Meerwein arylation;

References:

H?fling, Sarah B.;Hultsch, Christina;Wester, Hans-Jürgen;Heinrich, Markus R. [Tetrahedron,2008,vol. 64,# 52,p. 11846 - 11851] Location in patent:experimental part

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