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ChemicalBook CAS DataBase List 2-AMINO-4-CHLOROBENZOTRIFLUORIDE
445-14-7

2-AMINO-4-CHLOROBENZOTRIFLUORIDE synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: hydrogen fluoride; sulfur tetrafluoride / 24 h / 85 °C / Autoclave; Inert atmosphere
2: ammonium chloride; iron; hydrogenchloride / water; isopropyl alcohol / Reflux

References:

Alekseenko, Anatoliy N.;Bugera, Maksym Ya.;Gerus, Igor I.;Kiriakov, Oleksandr;Klipkov, Anton A.;Mykhailiuk, Pavel K.;Pustovit, Yurii;Razhyk, Bohdan;Semenov, Sergey;Starova, Viktoriia S.;Tananaiko, Oksana Yu.;Tarasenko, Karen;Tolmachev, Andrei A.;Trofymchuk, Serhii;Zaporozhets, Olga A. [Journal of Organic Chemistry,2020,vol. 85,# 5,p. 3110 - 3124]

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