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ChemicalBook CAS DataBase List 2,6-Pyridinedicarboxylic acid chloride
3739-94-4

2,6-Pyridinedicarboxylic acid chloride synthesis

4synthesis methods
Pyridine-2,6-dicarboxylic acid (105 mg, 0.52 mmol) mixed with 7mL of thionyl chloride was heated to reflux for 3 hours. After the excess thionyl chloride was removed, a white solid was obtained and used for the following synthesis without further purifications.
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: aq. KMnO4
2: SOCl2

References:

Kleigrewe, Nina;Steffen, Winfried;Bloemker, Tobias;Kehr, Gerald;Froehlich, Roland;Wibbeling, Birgit;Erker, Gerhard;Wasilke, Julia-Christina;Wu, Guang;Bazan, Guillermo C. [Journal of the American Chemical Society,2005,vol. 127,# 40,p. 13955 - 13968]

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