ChemicalBook CAS DataBase List 2,6-Pyridinedicarboxylic acid chloride

2,6-Pyridinedicarboxylic acid chloride synthesis

4synthesis methods

Product Name:2,6-Pyridinedicarboxylic acid chloride
CAS Number:3739-94-4
Molecular formula:C7H3Cl2NO2
Molecular Weight:204.01

Pyridine-2,6-dicarboxylic acid (105 mg, 0.52 mmol) mixed with 7mL of thionyl chloride was heated to reflux for 3 hours. After the excess thionyl chloride was removed, a white solid was obtained and used for the following synthesis without further purifications.

108-48-5 Synthesis

108-48-5
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3739-94-4
131 suppliers
$5.00/1g

Yield:-

Steps:

Multi-step reaction with 2 steps
1: aq. KMnO₄
2: SOCl₂

References:

Kleigrewe, Nina;Steffen, Winfried;Bloemker, Tobias;Kehr, Gerald;Froehlich, Roland;Wibbeling, Birgit;Erker, Gerhard;Wasilke, Julia-Christina;Wu, Guang;Bazan, Guillermo C. [Journal of the American Chemical Society,2005,vol. 127,# 40,p. 13955 - 13968]

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499-83-2 Synthesis