2(3H)-FURANONE,5-ETHYLDIHYDRO synthesis
- Product Name:2(3H)-FURANONE,5-ETHYLDIHYDRO
- CAS Number:2865-82-9
- Molecular formula:C7H12O2
- Molecular Weight:128.17
18479-51-1
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 76 percent / NBS / CCl4 / 18 h / 20 °C
2: potassium tert-butoxide / tetrahydrofuran; 2-methyl-propan-2-ol / 1 h / 50 - 60 °C
3: 85 percent / pyridinium chlorochromate / CH2Cl2 / 2 h / 28 °C / celite
References:
Baskaran, Sundarababu;Islam, Imadul;Chandrasekaran, Srinivasan [Journal of Organic Chemistry,1990,vol. 55,# 3,p. 891 - 895]
110-93-0
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